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논문 기본 정보

자료유형
학술저널
저자정보
Lee Minjeong (School of Materials Science and Engineering Gyeongsang National University) Kim Gyutae (School of Materials Science and Engineering Gyeongsang National University) Jeong Gyu Hyun (School of Materials Science and Engineering Gyeongsang National University) Yoon Aram (Department of Materials Science and Engineering Ulsan National Institute of Science and Technology) 이종훈 (울산과학기술원) Ryu Gyeong Hee (School of Materials Science and Engineering Gyeongsang National University)
저널정보
한국현미경학회 한국현미경학회지 한국현미경학회지 제52권 제1호
발행연도
2022.3
수록면
1 - 6 (6page)
DOI
10.1186/s42649-022-00076-z

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The process of encapsulating cobalt nanoparticles using a graphene layer is mainly direct pyrolysis. The encapsulation structure of hybrids prepared in this way improves the catalyst stability, which greatly reduces the leaching of non-metals and prevents metal nanoparticles from growing beyond a certain size. In this study, cobalt particles surrounded by graphene layers were formed by increasing the temperature in a transmission electron microscope, and they were analyzed using scanning transmission electron microscopy (STEM). Synthesized cobalt hydroxide nanosheets were used to obtain cobalt particles using an in-situ heating holder inside a TEM column. The cobalt nanoparticles are surrounded by layers of graphene, and the number of layers increases as the temperature increases. The interlayer spacing of the graphene layers was also investigated using atomic imaging. The success achieved in the encapsulation of metallic nanoparticles in graphene layers paves the way for the design of highly active and reusable heterogeneous catalysts for more challenging molecules.

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